Other - question about reaction/experiment

[Chefko]

A neighbour of a friend i know has some problems on a
try to cook some xmethx.
He took 5g Red P, 7g I2 and 4ml Dh20
and added 5g ephe hcl.temperature was raised slowly on
100-140 c and cooked and stirred a bit for 24 hours,after the 24 hours
the fluid was cooked 10 mins without kondensor to get rid of excess iodine,after that he added 75ml hot Dh20 and the fluid was filtered .
The colour of the fluid was nearlyand little little tint yellow.
he wasched the fluid with toluol(dry)one times.
after that the ph was raised on 12,5-14 (Naoh)and an extraktion 3x into toluol was made.
the toluol which should contain the baby was then wasched with fresh Naoh.after the seperation the toluol was added to fresh Dh20 and the
Ph was brought down on 8,seperated ,new water and the ph was brpoght down on 6,6 the 2 Dh20 which should now contain the baby in HCL Form
was evaporized under a heatinglamp,BUT SURPRISE there was nothing
after the DH20 evaporized.WHAT COULD BE HAPPENED TO THE BABY???
PLEASE GIVE SOME INFOS THE CONFUSION IS BIG!!!WAS SWIM PERHAPS SLOPPY???

[Spyder]

Please do not keep posting the same thing over and over!!!!!!

People will answer the question if they can.

For one thing, this is in the WRONG FORUM!!! It should be in the Newbie Chemistry Forum.

Second, SwiS already answered this question in swiYour other thread, which was exactly the same as this one!

Please have a look at the Forum Rules and also, try to put things into the proper forum, so others can benefit later.

S

[Chefko]

the problem is for a reason i can only put it in this forum,i would be happy if i could post in the chemisty forum,perhaps it is because im a "newbie"

[Spyder]

That is why it is called the NEWBIE CHEMISTRY FORUM!

SwiS is NOT talking about the Meth Chemistry Forum, Newbies cannot post there, but they CAN POST in the NEWBIE CHEMISTRY FORUM.

Even so, What does it help by posting the exact same thing many times?

SwiS is happy to help swiY all that he can, but come on, please, just try to have some respect for the site. When others try to search to get help later on, things like this get it all screwed up.

Check the other post of this same thing, swiS thinks he knows the problem.

S

PS: NOT A FLAME....Everybody is new sometime, just want swiYou to learn the right way now, so swiY will have no problems in the future.

For the record, this forum is about use/about/experiences/etc. of Methamphetamine, not manufacture/chemistry/etc.

S

[bmk]

after the reaction add 3 to 5 times the volume of water and run the mix through a filter to get rid of the red p (save it for the next run) then make the solution alkiline to PH 14-15 then extract with a solvent then seperate the two layers and add some hydrochloric acid to ph 7 and evap the tolulene and BAM meth left behind it is a good idea to give it a dry acatone wash at the end.DO NOT POST THIS AGAIN PLEASE.
allso the PH has to be nutral before the meth will drop from the water layer from the tolulene and ph 8 is still alkiline and after the tolulene pull why did swiy make it alkiline again? allso swiy might not have had clean E to start off with and got gaked thare are lots of reasons why a rxn can go wrong the mix was probebly a bit wet as well.

[Spyder]

Hey there swiBMK!, hope all is well...

actually solved this one in the other forum where it was posted....bad/gaaked E/pse!

swiHe only did a quick methanol pull.....on gaaked up pills...no surpise nothing at the end...

Take care..S