help please! - Drugs Forum
Drugs-Forum  
News Groups Blog Forum Chat Video Audio Images Documents Wiki Home
Go Back   Drugs Forum > CHEMICAL & (SEMI-) SYNTHETIC DRUGS > Research Chemicals
Register Tags Mark Forums Read

Notices

Research Chemicals Piperazines, Phenethylamines, Tryptamines & other Research Chemicals or designer drugs.

Reply
 
Thread Tools Display Modes
  #1  
Old 01-02-2005, 08:45
wslwh2005 wslwh2005 is offline
Account Awaiting Email Confirmation.
 
Join Date: 18-01-2005
Posts: 13
wslwh2005 is an unknown quantity at this point
Points: 57, Level: 1 Points: 57, Level: 1 Points: 57, Level: 1
Activity: 0% Activity: 0% Activity: 0%


after evaporation of the decalin under reduced pressure,the residue(ketamine) is extracted with dilute hydrochloric acid.


my question is how to use dilute hydrochloric acid to extracted the ketamine and the next step will be(describe in detaill)?


Reply With Quote
  #2  
Old 01-02-2005, 13:20
ChemicallyBound Gold member ChemicallyBound is offline
Gold Member
 
Join Date: 18-01-2005
Location: U.S.
Posts: 290
ChemicallyBound is an unknown quantity at this point
Points: 206, Level: 2 Points: 206, Level: 2 Points: 206, Level: 2
Activity: 0% Activity: 0% Activity: 0%
mix it with some dilute HCL (this is a fancy word, right? extracted)
Reply With Quote
  #3  
Old 02-02-2005, 03:56
diggitydawg diggitydawg is offline
Account Awaiting Email Confirmation.
 
Join Date: 28-01-2005
Location: United States
Posts: 26
diggitydawg is an unknown quantity at this point
Points: 51, Level: 1 Points: 51, Level: 1 Points: 51, Level: 1
Activity: 0% Activity: 0% Activity: 0%
so after mixing it you would have 2 separate layerswith the hcl / ketamine layer being on top?? wouldn't you just mix it for a while then centirfuge it and transfer that top layer......
Reply With Quote
  #4  
Old 02-02-2005, 14:09
ChemicallyBound Gold member ChemicallyBound is offline
Gold Member
 
Join Date: 18-01-2005
Location: U.S.
Posts: 290
ChemicallyBound is an unknown quantity at this point
Points: 206, Level: 2 Points: 206, Level: 2 Points: 206, Level: 2
Activity: 0% Activity: 0% Activity: 0%


no, he said:


after evaporation of the decalin under reduced pressure,the residue(ketamine) is extracted with dilute hydrochloric acid.


So: evaporation of the decalin under reduced press./ the residue:


means that there is no other solvent left, just mix the RESIDUE (w/o any solvent left b/c it was removed under reduced pressure) with dilute HCL. sounds pretty simple, if there is a layer it is stuff that doesn't go into solution in HCL...............................
Reply With Quote
Reply

Bookmarks

Thread Tools
Display Modes

Posting Rules
You may not post new threads
You may not post replies
You may not post attachments
You may not edit your posts

BB code is On
Smilies are On
[IMG] code is On
HTML code is Off

Forum Jump


Sitelinks: Site Functions:

All times are GMT +1. The time now is 07:10.


Copyright: Substance Information Network 2003 - 2009, All rights reserved