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Hashish & BHO Hashish, soap bar, resin, ice-o-lator, hash oil, bho, butane honey oil, butane hashish oil

 
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  #1  
Old 18-11-2009, 22:31
CoryInJapan CoryInJapan is offline
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Iso hash oil

Just thought I would show Swims results of a 24 hour soak in 91% isopropyl alcohol.

Swim did 2 more pulls

2nd pull was another 24 hours and resulted in about the same amount as the first pull.

3rd pull was sitting for about 30 hours and results were about a 3rd of the first pull.

So swim has concluded that 3-4 days max will get all the goodies out.

The first 2 pulls the alcohol turned so dark green it was almost black.
3rd pull the alcohol was pretty light green..almost see through.

Swim can say the full amount of oil that was because he doesnt have a scale.

But I think swim said the amount of cannabis put in was around 7-10 grams of shake and stems.


If that image dont show up Ill post it up again later.

CoryInJapan added 2 Minutes and 41 Seconds later...

Oh and incase you all were wondering if I had the pictures for the second and third pull. No, i do not.Swim didnt take any unfortunately.

Last edited by CoryInJapan; 18-11-2009 at 22:31. Reason: Automerged Doublepost
  #2  
Old 26-12-2009, 16:29
silentsoul silentsoul is offline
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Re: Iso hash oil

SWIM was wondering what kind of screening process SWIY used to remove the shake and stems that was mentioned. SWIM has a LOT of shake every several months that SWIM has always just thrown away. SWIM is tired of that and would like to take advantage of this TEK but needs further instructions. Also, SWIM checked checked some alcohol that he had and it seems it's only 70%, where might SWIM find 91% plus. Hell vodka is only 80%!?!?!?
  #3  
Old 26-12-2009, 21:13
rawbeer rawbeer is offline
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Re: Iso hash oil

Vodka is typically 80 proof which is 40%. 70% works fine, SWIM has used this same method with 70% and it works fine. He uses a fine jelly strainer - like a mesh basket - to filter. If you can find a flat glass dish it works best - rounded ones like the bowl shown here are harder to scrape.
You can let it evaporate or if you get impatient you can put it in an oven on like 250f and speed things up - make sure there's no flame inside the oven if you do this (the broiler could lead to a terrible accident with all those alc fumes). SWIM thinks three pulls is good - he's compared the quality of each pull seperately and after three there's no point.
If SWIY has a good connection for shwag this is a good way to make it worth smoking, or eating (you can just whip this stuff into a creamy pasta and it dissolves nicely.)

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nice way to get rid of that swag,
good comment about using a flat bottomed vessel
  #4  
Old 26-12-2009, 22:46
chilliker chilliker is offline
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Re: Iso hash oil

SWIM is currently doing this exact same thing with 70%.
  #5  
Old 26-12-2009, 23:22
silentsoul silentsoul is offline
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Re: Iso hash oil

SWIM doesn't drink much, sorry for the mistake. Good to know 70% works, will try soon SWIM says.
  #6  
Old 27-12-2009, 00:55
CoryInJapan CoryInJapan is offline
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Re: Iso hash oil

Swim used a metal sifter. Like the one you have in your kitchen, SEE BELOW. Then coffe filters to get the rest(which was mostly kief)

Its pretty simple. Good luck, hope swiy gets good results. I know swim did.

  #7  
Old 28-12-2009, 16:06
chilliker chilliker is offline
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Re: Iso hash oil

As SWIM mentioned he is doing this same TEK with some 70% ISO. When he used the coffee filter though the liquid wouldn't really go through it, but instead stayed on it like if it was non-porous. Also SWIM didn't get any Hash Oil but normal Hash instead, why is this?
  #8  
Old 28-12-2009, 16:54
rawbeer rawbeer is offline
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Re: Iso hash oil

SWIM thinks coffee filters are probably too fine - he never uses one, just the mesh screen.
The consistency of the product will vary - if you evaporate the alcohol completely the result will be gummy, but not quite 'oily', if this is what you mean.
  #9  
Old 28-12-2009, 17:56
CoryInJapan CoryInJapan is offline
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Re: Iso hash oil

Yea the only way it will be truelly oily is if swiy did the butane blast extraction.Iso hash oil is always more gummy like said before.
  #10  
Old 29-12-2009, 04:16
chilliker chilliker is offline
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Re: Iso hash oil

Quote:
Originally Posted by CoryInJapan View Post
Yea the only way it will be truelly oily is if swiy did the butane blast extraction.Iso hash oil is always more gummy like said before.
Is there any difference in the high?
  #11  
Old 29-12-2009, 05:52
yonez yonez is offline
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Re: Iso hash oil

swim suggests going down to your god ole' hydroponics store and investing in some 50/50 screen. works wonders for ISO oil.
  #12  
Old 29-12-2009, 14:19
anonuser30500 anonuser30500 is offline
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Re: Iso hash oil

Quote:
Originally Posted by chilliker View Post
Is there any difference in the high?
Possibly.

The butane extraction does not soak the material for long, just long enough to saturate it and then the butane, once it fills the extractor (honey bee extractor is a popular one) it immediately comes out again and brings all the THC resin out of the material.

This means less flavour and contaminants off the vegetative material would be in the finished product. It is likely as not purer than the iso extraction.

With the iso, some soak the material for a long time, and resoak it to leech all the resin. The flavour is different, maybe more harsh although both are fairly harsh if smoked in a UK joint.
  #13  
Old 29-12-2009, 17:03
CoryInJapan CoryInJapan is offline
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Re: Iso hash oil

Well swim never smoked any hash anything out of a joint as its a waist in swim opinion.

Swim smokes it out a special hash pipe and the only difference is the taste...Taste more chlorophylly but the high is identical for the most part.Honey oil taste better because if done right there will be very little or no chlorophyll.

Possibly the ISO oil has more cannabonoids in it.
  #14  
Old 13-03-2010, 14:43
silentsoul silentsoul is offline
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Re: Iso hash oil

SWIM started a 24 hour soak of 70% rubbing alcohol. But SWIM being his usual self, forgot about it until just now. Total soaking time was around 2.5 days that left the alcohol looking like a very dark greenish black color to it. SWIM is currently drying the left over alcohol in a small room that he's heating to about 85-95 degrees, hot but not too hot for the time it'll take to evaporate the alcohol. SWIM thinks it shouldn't take more than 24hrs or so. Wish swim luck, this was his first alcohol extraction.
  #15  
Old 13-03-2010, 15:54
CoryInJapan CoryInJapan is offline
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Re: Iso hash oil

Quote:
Originally Posted by silentsoul View Post
SWIM started a 24 hour soak of 70% rubbing alcohol. But SWIM being his usual self, forgot about it until just now. Total soaking time was around 2.5 days that left the alcohol looking like a very dark greenish black color to it. SWIM is currently drying the left over alcohol in a small room that he's heating to about 85-95 degrees, hot but not too hot for the time it'll take to evaporate the alcohol. SWIM thinks it shouldn't take more than 24hrs or so. Wish swim luck, this was his first alcohol extraction.
Swiy did everything fine and the end product will work as desired but,to get the best taste and least Impure oil is to use at least 91% if not 99% iso or everclear.

Also that means there is 30% water in there collecting more plant matter into the final products.

Swim personally would have coffee filtered it a couple times to try to get some out.

Though since swiy used 70% swim would have left it in there for 5 days instead of 3 days using 91%+

Though swiy should have got most of it anyways so it wont be that big a deal this time around/
  #16  
Old 13-03-2010, 17:10
silentsoul silentsoul is offline
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Re: Iso hash oil

Actually, SWIM made a pretty big mistake, he didn't rinse his 'trash' with fresh alcohol, he was thinking of doing a 24hr soak this time with the alcohol he's already added to the container and let it strain through a few coffee filters first. Gonna need a bigger plate though, what do SWIY use to hold all the liquid.
  #17  
Old 13-03-2010, 17:15
CoryInJapan CoryInJapan is offline
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Re: Iso hash oil

Quote:
Originally Posted by silentsoul View Post
Actually, SWIM made a pretty big mistake, he didn't rinse his 'trash' with fresh alcohol, he was thinking of doing a 24hr soak this time with the alcohol he's already added to the container and let it strain through a few coffee filters first. Gonna need a bigger plate though, what do SWIY use to hold all the liquid.
If Swiy means where do I hold all the liquid for evaporation? then he uses I large pyrex pie glass plate.

Mason jars for anything else.
He ended up picking up a pack of large mason jars for under 10 bucks and had like 12 mason jars.

Ever since then all his liqiud projects have been so much easier with all these mason jars.
  #18  
Old 13-03-2010, 19:53
silentsoul silentsoul is offline
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Re: Iso hash oil

How long should SWIM let his second run go? Remember, he didn't rinse the leftovers from the first. Just poured the alcohol through a little coffee filter type cup and that was it. SWIM was thinking of letting it set for 24hrs or so. Also remember that it's 70%, not 90%.
  #19  
Old 13-03-2010, 20:01
CoryInJapan CoryInJapan is offline
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Re: Iso hash oil

another 48 hours should get anything thats left or worth swiys time

Yea swim didnt rinse he did what swiy did but squeezed as much of the plant material that swim could.

then did a second extraction and swim got some good results still so 2 days is swims guess from experience.
  #20  
Old 14-05-2010, 00:09
Yail Bloor Yail Bloor is offline
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Re: Iso hash oil

My dear friend Dr. Raoul Duke is also mid-way through his own alcohol THC extraction. Having only ever extracted alkaloids from cactus, he fallowed the same proceedure he would with Peruvian Torch powder; soak powdered marijuana in 99% IPA, (marijuana filled 1/4 of the jar, IPA filled it to 3/4 total volume) for 3 days, shaking vigorously multiple times a day, decanted liquid layer, re-added fresh IPA to the same level, soak, shake, decant, repeat a third time. Dr. Duke plans to evaporate his extraction this weekend. However, he gathers, after reading this thread, that this length of time and number of pulls was probably unnessary, and possibly just served to extract more unwanted material. Can anyone confirm/deny Raoul's thinking? Do any SWIMmers have any advice, or a better way to do this in the future?

Edit: If it helps, Raoul used 9 grams marijuana, and probably 500 mls 99% IPA - so far anyway.

Last edited by Yail Bloor; 14-05-2010 at 00:12. Reason: added something
  #21  
Old 24-12-2010, 07:21
unknownid unknownid is offline
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Re: Iso hash oil

This is an old thread, but it is important to mention SWIY should NOT soak your weed in ISO over night. You will extract way more chlorophyl which is terrible for the taste and for the body.

SWIY should do a 20 - 30 second shake, and let it evaporate (in a pyrex dish in a pan if SWIY wants to speed up the evap process).
  #22  
Old 14-02-2011, 03:00
djneptunezjunglist djneptunezjunglist is offline
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Re: Iso hash oil

My good friend Cody's method for making "iso hash oil".

Materials Needed:
1 window screen
1 large bottle of 91% isopropyl alcohol
1 pair of rubber gloves
1 glass cooking dish
1 large clear plastic bottle with screw off top
clippings, stems, buds, and resin [if you must]
1 razor blade
A ventilated area [garage, outside, fan in window]

Here's what Cody had to say...

1] Start by cutting/breaking up all your buds/clippings and cut up your stems into .5"-1". You dont need to mince the clippings, just enough so theres more of it exposed.
2] Put the clippings/buds/resins into your container with a screw top.
3] pour in your isopropyl alcohol, enough to completely submerge everything in the container.
4] Shake it up nice and hard for 10 minutes every so often and let it soak for 24HRs.
5] After soaking it for 24 hours, give it another shake session for 5-10min.
6] Get your window screen and put on your rubber gloves.
7] Pour the liquid through the screen, make sure not to spill any clippings into the liquid. after all the liquid is poured through, squeeze the clippings/buds very hard like you're squeezing out water from a towel.
8] Now, you can just set it in front of a fan and let the alcohol evaporate, but this will take a few hours. Another way to get the alcohol to evaporate quicker is to put the glass cooking dish in boiling water. Use anything that your current glass dish will easily fit into without getting water in the iso liquid, or without spilling boiling water everywhere.
9] Now that all the alcohol is completely evaporated, get your razor blade and the rubber gloves again and scrape the product off the dish and into a pile.

Depending on what you materials you soaked, will determine how gooey the oil will be. Some of it might be very wet, and some might be bone dry.

If its really gooey, Cody suggests getting a razor blade or a knife and spreading the hash oil on a rolling paper, just like peanut butter, and then with marijuana roll a joint. excellent. Usually with this iso hash oil, when smoked on top of a bowel, it turns to liquid and after a little bit of smoking on it, it dries out.

If you don't have any bud to put underneath, you can put a glob of the iso oil on a little piece of rolling paper, fold it so its all covered up, and smoke that.

Hope this helps anyone.

Thanks.
Be safe, especially if you using boiling water!
  #23  
Old 14-02-2011, 20:44
unknownid unknownid is offline
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Re: Iso hash oil

Do not soak your iso over night people! Chlorophyll is a hell of a thing for swiy to ingest. 20 - 30 second shake is more than enough.

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Solid advice.
  #24  
Old 14-02-2011, 23:15
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Re: Iso hash oil

Quote:
Originally Posted by unknownid View Post
Do not soak your iso over night people! Chlorophyll is a hell of a thing for swiy to ingest. 20 - 30 second shake is more than enough.
Yes just a few minutes is plenty of time not over night. The thc filled tricombs brake down almost instantly with iso.
  #25  
Old 31-03-2011, 17:24
Mindless Mindless is offline
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Re: Iso hash oil

My Uncle Baldylocks is quite excited about his latest thought experiment. He imagined what would happen if he were given around 125 grammes of squidy black, which had turned out to be a bit weak and rather gritty when chewed. It would probably have been bulked up with soil or something similar. This substance was grated by hand with a cheese grater, then placed in the extraction jar with enough 99.9% Isopropyl alcohol to cover it. This was then processed with a hand blender.

The jar was shaken for around five minutes, then left to settle for a few minutes. The liquid was carefully poured through a mesh strainer lined with bamboo cloth, into a flat pyrex dish. The extraction process was repeated a second time, with this liquid being strained into the evaporation dish. A third extraction showed little yield. To speed up evaporation, the dish containing the oil bearing Iso was placed in an electric fan oven on 80 degrees centigrade, for 45 minutes. This was removed when still containing Iso ( to avoid burning the oil). Evaporation was allowed to continue over the next 24 hours. A smaller volume of oil bearing solvent would have evaporated faster, without the need to speed things up.

The oil looks just like any commercial hash oil; Baldylocks has been lucky in obtaining a lot of this over the years. The oil tastes authentic and is pretty strong. My Uncle Baldylocks would like to thank all of his peers at DF for making this possible, it seems like a small matter, but old Baldy has wanted to experiment with oil extraction for decades, and is delighted to have made this first rudimentary step.,




Last edited by Mindless; 30-04-2012 at 21:49. Reason: added image

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bho, bho extraction, butane hash oil, butane honey oil, cannabis extraction, cannabis extraction with butane, cannabis extraction with isopropyl alcohol, hash oil

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