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Re: Making Cocaine base w/ ammonia
SWIM forgot to add and this is extremely important that when doing the crytalization using ether, acetone, and HCl that everything be kept covered whenever possible and that everything be done whithout rest.
The Only time the wizard can rest is when base is drying or dried and bagged here is a more SWIM would say understandable way of explaining this 1. Cocaine in water (1g/60mL) 2. dilute ammonia in half or to about 10% whatever doesn't really matter. 3. pour in some ammonia and stir with non-porous rod (glass). Keep adding then stirring and adding then stirring until water no longer "paints" white when ammonia comes in contact. (as in the second picture above) 4. let base settle water should be clear. 5. pass through filter paper #2 and use some clean water to rinse off the base caught in the filter. if any base gets stuck on the sides of the jar use clean swoosh around and wash out onto the filter mass. 6. let drain and dry out. pressing the filter betwwen the hands will squeeze water through but the wizard runs the risk of pressing to hard and ripping the filter paper. air dry if fine just takes a long time. Now the wizard can rest Dry base is stable enough to have in bag for a long while without any penalty. When the wizard decides to form the HCl salt then he is not allowed to rest until finished Do in this order and remember it is VERY IMPORTANT to not do this with a HCl acetone solution that has been shelved for any amount of time. SWIM doesn't know why but the acetone will begin to turn yellow and does not produce desired results. 1. add dry base to ether (1g/15mL) 2. add 36-38% HCl Lab Grade if possible to acetone (.2mL/10mL) for every gram of base going to be crystalized. So [1g base/15mL Ether/10mL acetone/.2mL HCl] 3. add HCl/acetone solution all at once to base/ether solution. immediately it turns white as milk then crytals begin to settle 4. when all crystals settle and the ether looks completely transparent then slowly swoosh crystals around and pass through funnel shaped filter paper makig sure tho catch the ether undrneath in a clean dry jar. 5. pass some clean acetone over crytals in the filter and also collect in the jar. 6. dry out by fanning with unheated air. (NO HOT AIR BLOW DRYING!!!!) 7. a small electric fan works well. Just far enough away so that no crystals fly out. 8. Drying is determined when a piece can be placed on a mirror and easily powders up. if the caine gets clumped up then it is still "ether wet" Also even if it doesn't seem to matter the relative humidity when doing the crystaliztion greatly affects the outcome. The lower the relative humidty is in the wizards room the better. water is a bad thing in this process. Last edited by Deckstruct 11; 07-04-2007 at 11:36. |
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